Library · Materials, chemistry & fabrication

What Laser Sintering & Ablation got wrong, from 42 theses

Summary written by a model from the records below: The records document numerous experimental failures and design rejections across laser sintering, selective laser melting, laser additive manufacturing, and laser ablation processes. Performance breakdowns typically stem from suboptimal laser fluence, excessive thermal accumulation, ablative debris deposition, residual thermal stress, and chaotic melt pool dynamics. These records come from graduate theses, 2021 to 2026, each labeled with its degree where the repository states it, and each links to its thesis. They were extracted by language models reading the full text, so treat each as a lead to read, not a verdict.

42
theses
17
institutions
48
failure records
6
failure modes

Plus 9 problems the authors left open, listed at the end.

Failure modes, by theses reporting them

Select a mode to jump to its records.

Excessive thermal input and energy concentration cause overheating, melting, or charring of targets
11
11 theses · 8 institutions · 12 records
Sub-threshold laser power and insufficient fluence lead to incomplete melting and lack of fusion
9
9 theses · 5 institutions · 10 records
Laser processing exhibits lower throughput, slower removal rates, or inferior fidelity relative to baseline methods
7
7 theses · 6 institutions · 7 records
Ablative debris redeposition and recast accumulation degrade feature resolution and surface quality
7
7 theses · 4 institutions · 8 records
Thermal stresses and thermal expansion mismatches induce severe cracking and part distortion
6
6 theses · 5 institutions · 6 records
Melt pool instabilities, plume interference, and keyholing disrupt additive deposition
5
5 theses · 3 institutions · 5 records

Excessive thermal input and energy concentration cause overheating, melting, or charring of targets

11 theses · 8 institutions

High laser intensities, low traverse speeds, and multi-photon absorption deliver uncontrolled thermal energy that overheats sensitive substrates. This leads to complete powder bed melting, component charring, structural buckling, and violent disruptions of underlying materials.

Tried and failed

selective laser sintering with high thermal input applied to polymeric solid dispersion powder beds. Outcome: unstable. Reason: low laser speed and high bed temperature caused excessive energy density and complete powder bed melting

Expanding the processing space for amorphous solid dispersions · UT Austin · PhD

Tried and failed

Below-bandgap femtosecond laser writing applied to suspended semiconductor nanostructures. Reason: Nonlinear absorption caused structural melting and ablation of suspended cavities even at low pulse energies.

Formation, integration, and control of semiconductor spin-defects in electronic and photonic devices · Harvard · PhD

Tried and failed

increasing laser pulse energy for particle acceleration applied to laser-driven microparticle acceleration. Reason: direct ablative heating and optical saturation caused particle fracture or melting rather than higher velocity

High-Velocity Microparticle Impact for Analytical Modelling of High-Strain-Rate Mechanics and Material Behavior · MIT · PhD

Tried and failed

ultrafast laser structuring of polymer particles applied to polystyrene microspheres. Reason: low melting point caused thermal damage and melting rather than deep ablation

Large-scale multifunctional bio-inspired nanostructures and their process modeling enabled by optical emission spectroscopy · UT Austin · PhD

Considered and rejected

Considered and rejected: Rejected below-bandgap femtosecond laser writing because multi-photon absorption delivered excessive instantaneous power that melted suspended nanostructures.

Formation, integration, and control of semiconductor spin-defects in electronic and photonic devices · Harvard · PhD

Considered and rejected

Considered and rejected: Rejected using a constant 500 W laser power across all 10 layers for thin wall fabrication due to excessive heat accumulation and remelting of previous layers reducing deposition efficiency.

Investigation of wire-based laser directed energy deposition (DED) process for high-resolution submillimetre features · Cranfield · PhD

Tried and failed

laser cutting thin polymer adhesive sheets applied to microfluidic channel and electrode cavity patterning. Reason: low laser power caused incomplete cutting while high power or low speed caused thermal burnout

Design and Fabrication of Microfluidic Electrochemical Sensor for Lead Detection in Drinking Water · York University · Master's

Tried and failed

laser sintering at high power and speed applied to dispensed conductive silver paste traces. Reason: excessive thermal input charred and embrittled the conductive traces

Computational Fabrication and Assembly for In Situ Manufacturing · MIT · PhD

Tried and failed

laser ablation of conductive coatings applied to silicone elastomer membranes. Outcome: worse than baseline. Reason: laser thermal energy caused localized substrate surface stiffening, preventing recovery of original mechanical compliance

Multifunctional Dielectric Elastomer Actuator for in vitro Cell Mechanostimulation · EPFL · PhD

Considered and rejected

Considered and rejected: Rejected printing 3D dielectric microstructures directly on top of metal vias/traces because direct laser absorption heats the metal and violently disrupts the print.

Novel entangling gates and scalable trap designs for trapped-ion quantum computing · University of Oregon · PhD

Tried and failed

CO2 laser cutting applied to thin silicone elastomer sheets. Reason: Photothermal ablation caused thermal buckling and edge charring, leading to channel misalignment and fluid leakage

A biocubesat compatible payload for future space systems: development of a second generation bammsat payload for stratospheric balloon flight · Cranfield · PhD

Tried and failed

Single-exposure high-intensity ultrafast laser photopolymerisation applied to 3D optical metamaterial microfabrication. Outcome: unstable. Reason: High laser intensities triggered avalanche photopolymerisation, causing uncontrolled bubbling, porosity, and loss of microscale features

Spatio-temporal light shaping for metamaterials · Imperial · PhD

Sub-threshold laser power and insufficient fluence lead to incomplete melting and lack of fusion

9 theses · 5 institutions

Operating lasers below critical power thresholds, with excessive scanning speeds, or with short exposure times fails to deliver the energy required for complete melting or curing. Consequently, parts suffer from lack-of-fusion porosity, unbonded powder layers, incomplete via drilling, and loose sintering.

Tried and failed

low power with reduced hatch spacing applied to laser powder bed fusion. Outcome: worse than baseline. Reason: Lack-of-fusion porosity at meltpool boundaries caused brittle cleavage despite achieving finer grain size

Digital Twins for Accelerated Qualification in Additive Manufacturing · Virginia Tech · Doctorate

Tried and failed

low repetition frequency laser processing applied to metal powder bed fusion. Reason: energy density threshold required for complete melting was not reached, causing only loose sintering

Multiple-material selective laser melting process development : advancements in the deposition and characterization of multiple-material interfaces · UT Austin · PhD

Tried and failed

selective laser melting with short exposure time applied to aluminum alloy additive manufacturing. Reason: insufficient energy input from large melt cross-section and short exposure time caused lack of fusion

Characterization of Heat Exchange for Additively Manufactured Components · York University · PhD

Tried and failed

laser ablation for microvia drilling applied to polymer dielectric build-up layers. Reason: insufficient laser energy prevented full dielectric ablation in small diameter via holes

Heterogeneous Integration for High-Speed mm-Wave Communication · Georgia Tech · PhD

Tried and failed

low pulse energy annular laser ablation applied to tissue microbiopsy harvesting. Reason: energy density below threshold failed to reliably eject intact tissue samples

Laser beam shaping for surgery and microbiopsy · UT Austin · PhD

Tried and failed

pulsed laser deposition at low pulse energy applied to oxide thin film deposition. Reason: insufficient laser fluence caused non-uniform island growth rather than continuous layer-by-layer film growth

Epitaxial Strain of Rare-Earth Nickelates on STO Using Pulsed Laser Deposition · UT Austin

Tried and failed

laser powder bed fusion at low power applied to refractory metals. Reason: laser power below threshold failed to achieve complete melting regardless of normalized enthalpy

Development of Materials for Extreme Environment Applications by Laser Powder Bed Fusion · MIT · PhD

Tried and failed

low-power laser thermal sintering applied to conductive silver paste traces. Reason: laser power was insufficient to reach the required curing temperature

Computational Fabrication and Assembly for In Situ Manufacturing · MIT · PhD

Tried and failed

High-speed laser sintering applied to conductive silver paste traces. Reason: Fast scan speeds limit thermal penetration depth, leaving subsurface material uncured regardless of applied power

Computational Fabrication and Assembly for In Situ Manufacturing · MIT · PhD

Tried and failed

selective laser melting at low power applied to thermoelectric powder sintering. Reason: laser power was insufficient to heat the melt pool above the required sintering temperature

Numerical Analysis of the Melt Pool Kinetics in Selective Laser Melting Based Additive Manufacturing of M g2Si Thermoelectric Powders · Virginia Tech · Master's

Laser processing exhibits lower throughput, slower removal rates, or inferior fidelity relative to baseline methods

7 theses · 6 institutions

Laser ablation and sintering often achieve significantly lower material removal rates and higher processing times than conventional mechanical drilling or milling. Furthermore, laser direct-write and liquid ablation strategies frequently demonstrate reduced etch efficiency, higher spatial variation, and worse resolution compared to baseline techniques.

Lost to a baseline

Parallel line laser sintering resulted in ~70% corner-to-center variation, performing worse than standard thermal sintering (17%) and IPL sintering (5.4%).

Inkjet-Printed Conductive Electrodes: Design, Fabrication, and Characterization · York University · PhD

Considered and rejected

Considered and rejected: Laser ablation from metallic foil rejected due to material waste from subtractive processing and lower throughput compared to additive printing.

Biodegradable and printed chipless environmental sensors for sustainable Internet-of-Things applications · EPFL · PhD

Tried and failed

temporal pulse splitting with long intervals applied to laser ablation of hard mineral deposits. Outcome: worse than baseline. Reason: second-scale inter-pulse delays failed to replicate the thermal or cavitation advantages of microsecond pulse modulation

Laser beam shaping for surgery and microbiopsy · UT Austin · PhD

Lost to a baseline

Laser ablation bone removal rate of ca. 2.88 mm3/min was ~165x slower than conventional drilling (477 mm3/min) for equivalent volume removal, with significantly higher cumulative heat exposure

Bone: A study of machining-induced damage and the role of interstitial fluid · Nottingham · PhD

Lost to a baseline

At 44 MPa in RBC phantoms, 1 Hz PRF achieved higher ablation efficiency than 2500 Hz PRF ("complete ablation. in 540±28 pulses for 1 Hz PRF in comparison with 655±19 pulses at 2500 Hz").

High-Rate Histotripsy Methods for the Rapid Removal of Soft and Fibrous Tissue · Virginia Tech · Doctorate

Lost to a baseline

Visible meta-optics fabricated with laser direct-write (HiRes) exhibited lower resolution and patterned shell-like artifacts compared to electron beam lithography (JEOL JBX6300FS).

MEMS-integrated Alvarez Metalenses and Large-area Meta-optics · University of Washington · PhD

Ablative debris redeposition and recast accumulation degrade feature resolution and surface quality

7 theses · 4 institutions

Material vaporized or ejected during pulsed laser ablation frequently redeposits onto nearby features and optical setups. This redeposited material creates raised edge lips, recast accumulation within micro-grooves, excessive surface roughness, and contaminated via channels.

Considered and rejected

Considered and rejected: Rejected complex multi-directional femtosecond laser raster patterns in favor of a simplified pattern to decrease ablated debris redeposition and wall taper.

Understanding Degradation Mechanisms of Metallic Alloys in High-Temperature Molten Salt Environments · Georgia Tech · PhD

Considered and rejected

Considered and rejected: Rejected upright reflected light microscopy on the femtosecond laser setup in favor of an inverted design to reduce debris re-deposition during laser ablation.

Multifunctional Polymer Fiber Probes for Biomedical Application · Virginia Tech · Doctorate

Tried and failed

excimer laser ablation micromachining applied to fused silica cavity fabrication. Outcome: too slow. Reason: produced excessive surface roughness and required prohibitive sequential processing times for millimeter-scale cavity milling

The Development Of A Fingertip Implantable Mems Tactile Sensing System · Penn · PhD

Tried and failed

static micro-beam pulsed laser surface ablation applied to metal surface micro-structuring for hybrid joining. Outcome: worse than baseline. Reason: Low scan speeds and small beams caused recast accumulation, groove blockage, and internal voids.

Theoretical and Experimental Investigation of Ultra High-Strength Joining in Steel-Short Fiber Reinforced Composites · Georgia Tech · PhD

Tried and failed

single-step laser ablation applied to substrate cavity micromachining for direct bonding. Reason: laser ablation created a raised redeposited edge lip that disrupted wafer direct bonding

The Development Of A Fingertip Implantable Mems Tactile Sensing System · Penn · PhD

Tried and failed

laser drilling apertures applied to stainless steel substrates. Outcome: worse than baseline. Reason: produced imprecise, damaged, and uneven crater-like edges compared to mechanical drilling

Coherent charge dynamics in molecules on the attosecond to few-femtosecond timescale · Imperial · PhD

Tried and failed

UV laser ablation of microvias applied to high-melting-point dielectric polymer films. Reason: High melting temperature caused irregular via shapes, excessive debris, and severe post-clean film thinning

Design and Demonstration of Mechanical and Electrical Reliability of 1-micron Redistribution Layers · Georgia Tech · PhD

Tried and failed

semi-additive processing with through-dielectric vias applied to ultra-low-k polymer interconnect redistribution layers. Reason: Laser debris, non-uniform electroplating, and seed-etch dielectric damage compromised via-containing conductor lines

Reliability Assessment and Demonstration of Ultra-low-k Dielectric Materials for Advanced Interposers · Georgia Tech · PhD

Thermal stresses and thermal expansion mismatches induce severe cracking and part distortion

6 theses · 5 institutions

Rapid heating and cooling cycles create large residual stresses and thermal expansion mismatches in laser powder bed fusion and micromachining. These localized stresses cause thin-walled features to warp, produce bulging hole profiles, and trigger substrate cracking or detachment during recoating.

Tried and failed

laser powder bed fusion additive manufacturing applied to fine internal channels and thin-walled features. Reason: feature resolution limits caused internal channel blockage and thin-wall cracking during fabrication

ADDITIVELY MANUFACTURED INSTRUMENTATION FOR ENHANCED FLOWFIELD MEASUREMENT IN A TRANSONIC AXIAL COMPRESSOR · Naval Postgraduate School · Master's

Tried and failed

laser powder bed fusion additive manufacturing applied to sub-millimeter thin wall fabrication. Reason: residual stress and thermal warpage caused recoater-part collisions below 500 µm feature sizes

Multi-Scale Materials Characterization and Analysis of In-Situ Process Monitoring Data towards enabling Multivariate Statistical Process Control in Laser Powder Bed Fusion Metal Ad · Georgia Tech · PhD

Considered and rejected

Considered and rejected: Laser cutting and continuous welding were rejected in favor of EDM wire cutting and pulse-spot welding to minimize residual stress and edge material degradation.

Novel Permeance–Based Equivalent Circuit Model for Improved Performance Prediction of Traction Induction Motors in Electric Vehicles · University of Windsor · PhD

Tried and failed

laser milling thin microwave dielectric substrates applied to millimeter-wave reconfigurable patch antennas. Reason: Laser micromachining caused substrate cracking and degradation in thin laminates, degrading bandwidth and polarization performance

mm-Wave Reconfigurable Antenna Systems for 5G Applications · Georgia Tech · PhD

Tried and failed

high-power pulsed laser machining with spiral toolpath applied to chemical vapor deposition diamond drilling. Reason: excessive thermal stress and ablation induced bulging hole profiles and substrate cracking

Advances in Instrumentation for Dynamic Nuclear Polarization & Magic-Angle Spinning NMR · MIT · PhD

Tried and failed

laser powder bed fusion on dissimilar substrates applied to copper-steel dissimilar metal printing. Reason: thermal expansion coefficient mismatch caused severe thermal accumulation, substrate distortion, and interfacial cracking

Enhancing laser powder bed fusion processability of copper with nanocoated powder and in-situ monitoring · Imperial · PhD

Melt pool instabilities, plume interference, and keyholing disrupt additive deposition

5 theses · 3 institutions

Small laser spot sizes and aggressive energy inputs push additive melt pools past keyhole thresholds, causing metal vaporization, spatter, and severe undercutting. In addition, vapor plume interference, plasma bursts, and gas interactions lead to wandering laser beams, nozzle clogging, and unstable droplet transfer.

Tried and failed

reducing laser beam spot size with wire feed applied to laser additive manufacturing. Outcome: unstable. Reason: Excessive peak power density caused plume interference, wire deviation, and lack-of-fusion defects.

Investigation of wire-based laser directed energy deposition (DED) process for high-resolution submillimetre features · Cranfield · PhD

Tried and failed

focused laser beam for secondary melt pool reshaping applied to wire directed energy deposition. Outcome: unstable. Reason: small spot sizes exceeded keyhole threshold causing metal vaporisation, severe undercut, and spatter

Bead shape control using multi-energy source (mes) for wire-based directed energy deposition (ded) process. · Cranfield · Doctorate

Tried and failed

argon shielding gas in laser powder bed fusion applied to stainless steel additive manufacturing. Outcome: unstable. Reason: induced plasma bursts and laser beam wandering, causing chaotic transitions between keyhole and conduction melting regimes

Effect of different shielding conditions, thermal cycles and post- deposition treatments on melting behaviour and mechanical properties of additively built components · Cranfield · PhD

Considered and rejected

Considered and rejected: Operating at variable laser power settings, rejected to prevent fourth-parameter confounding, thermal lensing, mode instability, and plume debris optical contamination.

A Process-Development Framework for UV-Laser Through-Silicon Via Drilling in Semiconductor Packaging · Johns Hopkins · Master's

Considered and rejected

Considered and rejected: Rejected high-density parameter sets with low traverse rates and high laser powers due to excessive nozzle balling and clogging.

DIRECTED ENERGY DEPOSITION PROCESSING OF ALPHA-BETA, NEAR-ALPHA, AND BETA TITANIUM ALLOYS · Dalhousie · Master's

Left open by the authors

Problems the authors named and did not get to.

Left open

Mitigate microcracks and intermetallic disconnections in selective laser melted Finemet soft magnetic alloys. Blocker: Requires additive manufacturing lab equipment (selective laser melting machine) and material characterization tools.

Selective Laser Melting of Finemet Soft Magnetic Material · Virginia Tech · Master's

Left open

Determine whether small thermal shock cracks heal post-scanning during final densification sintering of 8-YSZ. Blocker: Requires a physical materials laboratory, sintering furnace, laser flash sintering apparatus, and characterization equipment (e.g., SEM).

Control of selective laser flash sintering of yttria-stabilized zirconia · UT Austin · PhD

Left open

Perform high cycle and low cycle fatigue testing and crack propagation analysis on 3D printed gradient 316L stainless steel specimens. Blocker: Requires selective laser melting 3D printing equipment and physical mechanical/fatigue testing apparatus

3-D Printing, Characterizing and Evaluating the Mechanical Properties of 316L Stainless Steel Materials with Gradient Microstructure · Virginia Tech · Master's

Left open

Optimize selective laser melting parameters and analyze substrate positioning to reduce density variation in Finemet alloy parts. Blocker: Requires a selective laser melting physical apparatus and Finemet alloy powder to perform experimental builds

Selective Laser Melting of Finemet Soft Magnetic Material · Virginia Tech · Master's

Left open

Apply selective laser sintering to directly process binderless low-temperature phase ceramics like boehmite to initiate phase transitions and particle necking. Blocker: Requires physical selective laser sintering (SLS) apparatus and ceramic powder materials (boehmite).

Indirect selective laser sintering of ceramics · UT Austin · PhD

Left open

Study elongated cell, melt pool, and grain formation during selective laser melting of 316L stainless steel. Blocker: Requires a selective laser melting 3D printer and microscopy/metallurgical characterization equipment.

3-D Printing, Characterizing and Evaluating the Mechanical Properties of 316L Stainless Steel Materials with Gradient Microstructure · Virginia Tech · Master's

Left open

Evaluate residual stress and texture of LPBF Fe-Si alloys (>6 wt% Si) using alternative scan strategies to achieve crack-free parts. Blocker: Requires a Laser Powder Bed Fusion (LPBF) additive manufacturing machine, metal powders, and physical characterization equipment (e.g., XRD/EBSD).

Optimisation of silicon content in Fe-Si alloys processed via Laser Powder Bed Fusion for an additively manufactured soft magnetic core Laser Powder bed fusion of Fe-Si alloys and · Nottingham · PhD

Left open

Test additively manufactured SLM pool boiling surfaces with spherical re-entrant cavities across varying geometric parameters. Blocker: Requires selective laser melting (SLM) additive manufacturing and experimental pool boiling testing apparatus

Characterization of Heat Exchange for Additively Manufactured Components · York University · PhD

Left open

Apply additive manufacturing microstructural control methods to Ti-based, CoCrMo, and Al alloys for tailored tribological properties. Blocker: Requires selective laser melting (SLM) additive manufacturing equipment, specialized metal alloy powders, and characterization tools (SEM, EBSD).

Additive manufacturing: Towards alloys with spatially defined tribological properties · Imperial · PhD

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